Advances in Sintering Science and Technology II: Ceramic by Suk-Joong L. Kang, Rajendra Bordia, Eugene A. Olevsky,

By Suk-Joong L. Kang, Rajendra Bordia, Eugene A. Olevsky, Didier Bouvard

This booklet presents an exceptional one-stop source for figuring out crucial present matters within the examine and advances in sintering technology and technology.Content:

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The microstructural characterization was carried out by SEM, TEM, and XRD. The results showed the formation of a precursor SrMo04 phase in powders analyzed after mechanical ball milling process. On the other hand, analysis of samples calcinated for 2 h confirmed the existence of SrMo04 and Sr2Fe20s phases which are precursors of the Sr2FeMo06 compound. χ Οβ compound after the reduction process. The phase structure of the double perovskite was confirmed by Transmition Electron Microscopy. INTRODUCTION Double perovskite compounds have attracted intense research activities in both theoretical and applied areas of solid state physics and materials science due to their interesting structural, magnetic and electronic properties.

DB Voi% (b) B/A-B i J vom (c) R/A Fig. 2. 3. Reaction Rate and Water absorption According to Dosages of C/B and A/C In order to identify the impact of foaming of the aggregate according to the reaction rate difference between C/B and A/C, DTG analysis was performed and the results were as illustrated in Fig. 3. Heating rates are 5°C, 10°C, 15°C, 20CC per minute, respectively. Based on the DTG results, reaction constant k was calculated and listed in Table 4. As shown in Fig. 3, the case of C/B addition showed a rapid response regardless of the rate of temperature increase, compared to the case of A/C addition.

This corresponds to the end of the silica reduction since the mass loss rate becomes constant and is deduced by putting rr = 0 in Eq. 3: Am AI ' s« RTx:f (4) o For the Φ 15 sample, the global mass loss is higher since the sample mass and thus the amount of silica to be reduced is also higher. A sudden collapse in the mass loss rate 48 · Advances in Sintering Science and Technology II Sintering of Silicon, Effect of the Sample Size on Silica Reduction Kinetics and Densification associated with a complete silica reduction is also predicted by the model.

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